Asymmetric Synthesis of (−)-Pterocarine and (−)-Galeon via Chiral Phase Transfer-Catalyzed Atropselective Formation of Diarylether Cyclophane Skeleton.

DOI Number:

10.1021/acs.orglett.7b00570

Reaction Category:

MOP ID:

MOP_0000561

Educt:

2-substituted 5-(7-(4-fluoro-3-nitrophenyl)alkyl)-phenol

Product:

(31Z,33Z)-16-substituted-32-nitro-2-oxa-1(1,3)-benzena-3(1,4)-cyclohexanacyclophane-31,33-diene--ethane (1/1)

Catalyst:

1-[[3,5-bis(trifluoromethyl)phenyl]methyl]-9-hydroxy- (9S)-Cinchonanium bromide (1:1)

Cas No:

947508-14-7

Cas No:

118-10-5